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| 布雷德奈克試劑的典型應(yīng)用（1） |
| 2022-06-19 |
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Methylterephthalonitrile (1.42g, 9.99mmol) and Bredereck's reagent (3.48g, 19.98mmol) were dissolved in DMF (15mL).
The reaction mixture was heated at 75°C under nitrogen for 72hrs after which time the solvent was removed in vacuo.
Trituration with Pet. Ether gave a bright yellow solid identified as 2-((E)- 2-dimethylamino-vinyl)-terephthalonitrile ester (1.88g, 0.95mmol, 95% yield)
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